THE MADURAI DIRAVIYAM THAYUMANAVAR HINDU COLLEGE

HINDCO RESEARCH JOURNAL

ARTICLE NAME:
Studies on the growth, structural, optical, mechanical and dielectric properties of 4-Aminopyridinium oxalate single crystals

AUTHOR NAME
K. Balasubramanian, A. Ponchitra

ISSUE:
VOL.1, NO.2

YEAR:
2018

PAGE NO:
212-217

ABSTRACT:
4-Aminopyridinium oxalate is an organic crystal has been grown by slow evaporation solution growth technique. The solubility of the 4-Aminopyridinium oxalate crystal increases with increasing temperature. The structure of 4-Aminopyridinium oxalate is confirmed by single crystal X-ray diffraction method. The title compound crystallizes in the monoclinic system and the space group is C2/c. The presence of various functional groups in the grown crystal is identified from FTIR analysis. The optical property such as transmittance of the grown 4-Aminopyridinium oxalate crystal is obtained from UV-Visible spectroscopic studies. The mechanical stability of the grown crystal has been studied by using Vickers microhardness test and it reveals that the 4-Aminopyridinium oxalate crystal is the soft category material. The dielectric constant and the dielectric loss of the specimen were also studied.

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